HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Bromo-3-methoxypropane → 1-[3-Tert-butyl-4-methoxy-5-(3-methoxypropoxy)phenyl]ethanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Bromo-3-methoxypropane | HCID 524551 | — |
| Reactant | 1-(3-Tert-butyl-5-hydroxy-4-methoxyphenyl)ethanone | HCID 58136946 | — |
| Product | 1-[3-Tert-butyl-4-methoxy-5-(3-methoxypropoxy)phenyl]ethanone | HCID 58046024 | 56.6% |
Reaction Steps
1-(3-tert-Butyl-5-hydroxy-4-methoxyphenyl)ethanone (O3.070; 2.00 g) and 1-bromo-3-methoxypropane (1.65 g) were converted, worked up and purified analogously to O2.110. 1.50 g of the title compound were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076336B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-cb5017dc1e7140219b08dd73446aecb9 |
| Source note | uspto-grants-2011_12 |