HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diazomethane → Methyl 3,5-Dibromobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diazomethane | HCID 9550 | — |
| Reactant | Benzoic acid, 3,5-dibromo- | HCID 12063 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Methyl 3,5-Dibromobenzoate | HCID 621923 | — |
Reaction Steps
To a solution of 3,5-dibromobenzoic acid (1 eq.) in ether was added dropwise a solution of diazomethane in ether until gas evolution had ceased. The reaction was stirred for 20 min and concentrated in vacuo to afford the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076359B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-c9c0b78b58ea4da49f17993ef5b5aaae |
| Source note | uspto-grants-2011_12 |