HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylaldehyde → N,N'-Dodecamethylenebis(2-hydroxybenzylamine)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylaldehyde | HCID 6998 | — |
| Reactant | 1,12-Dodecanediamine | HCID 17727 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Isopropanol | HCID 3776 | — |
| Product | N,N'-Dodecamethylenebis(2-hydroxybenzylamine) | HCID 4535168 | — |
Reaction Steps
30.0 g of a bisazomethine prepared from 2 mols of salicylaldehyde and 1 mol of 1,12-diaminododecane and having a melting point of 72°-73° C. are hydrogenated for 2 hours in 300 ml of isopropanol in an autoclave in the presence of 3 g of Raney nickel at 90°-100° C. and under a pressure of 60 atmospheres
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04129556 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-9057bde9aaa04913b95b1cd6bdea6ee3 |
| Source note | uspto-grants-1978_12 |