HCID 24765046, compound → HCID 24765047, compound

Participants

Reaction Steps

A solution of 3-{4-[1-(2,6-dimethyl-4′-trifluoromethyl-biphenyl-4-yloxymethyl)-cyclopent-3-enyl]-benzoylamino}-propionic acid (0.134 g, 0.250 mmol) in EtOH (3.0 mL) is treated with 10% palladium on carbon (26.7 mg), flushed with hydrogen, and stirred under 1 atm pressure overnight. The mixture is then filtered through Celite® and concentrated to provide 0.0350 g (26%) of the title compound as a clear syrup. MS (ES): 540.4 [M+H]+.

Provenance & Evidence