HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-fluorophenol → 5-Amino-2-fluorophenol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-fluorophenol | HCID 2724981 | — |
| Reactant | 3-Amino-4-fluorophenol | HCID 13519180 | — |
| Product | 5-Amino-2-fluorophenol | HCID 22641413 | 86% |
Reaction Steps
This compound was prepared from 4-bromo-2-fluorophenol (3.0 g, 15.71 mmol) in the manner described for 3-amino-4-fluorophenol, affording 1.79 g (86%) of 3-amino-6-fluorophenol. 1H-NMR (DMSO-d6) δ 10.42 (s, 1H), 9.69 (br s, 2H), 7.22 (dd, J=8.4, 6.6 Hz, 1H), 6.93 (dd, J=5.7, 2.1 Hz, 1H), 6.74 to 6.99 (m, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076488B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-0a060ac099634d6e8f6dfe7ee32c9dd8 |
| Source note | uspto-grants-2011_12 |