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HRID658544

反应详情

EQUATION

反应方程式

HRID 658544 的结构方程式

REACTANTS

反应物

2
结构：CON(C)C(=O)[C@@H](Cc1ccccc1F)NC(=O)OC(C)(C)C
HCID59799859

未命名化合物

结构：Cc1cc(F)ccc1C(=O)NC(C)(C)C
HCID59804558

N-(1,1-Dimethylethyl)-4-fluoro-2-methylbenzamide

C12H16FNO

PRODUCTS

生成物

1
结构：CC(C)(C)NC(=O)c1ccc(F)cc1CC(=O)[C@@H](Cc1ccccc1F)NC(=O)OC(C)(C)C
HCID69109421

未命名化合物

PROCEDURE

实验过程

Using general procedure 2 with [(R)-2-(2-Fluoro-phenyl)-1-(methoxy-methyl-carbamoyl)-ethyl]-carbamic acid tert-butyl ester (1.6 g, 3.9 mmol) and N-tert-Butyl-4-fluoro-2-methyl-benzamide (3.0 g, 14 mmol) followed by purification by silica gel flash column chromatography gives the title compound.

WORKUP

后处理

  1. customfollowed by purification by silica gel flash column chromatography