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HRID658547

反应详情

EQUATION

反应方程式

HRID 658547 的结构方程式

REACTANTS

反应物

2
结构：Cc1cccc(C)c1C(=O)NC(C)(C)C
HCID19699668

N-tert-Butyl-2,6-dimethylbenzamide

C13H19NO

结构：CON(C)C(=O)[C@@H](Cc1ccccc1F)NC(=O)OC(C)(C)C
HCID59799859

未命名化合物

PRODUCTS

生成物

1
结构：Cc1cccc(CC(=O)[C@@H](Cc2ccccc2F)NC(=O)OC(C)(C)C)c1C(=O)NC(C)(C)C
HCID69108516

未命名化合物

PROCEDURE

实验过程

Using general procedure 2 with [(R)-2-(2-fluoro-phenyl)-1-(methoxy-methyl-carbamoyl)-ethyl]-carbamic acid tert-butyl ester (2.65 g, 8.1 mmol) and N-tert-butyl-2,6-dimethyl-benzamide (5.0 g, 24 mmol), followed by purification by silica gel flash column chromatography gives the title compound.

WORKUP

后处理

  1. customfollowed by purification by silica gel flash column chromatography