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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 658617Generated: October 31, 2026

Phenethylamine → HCID 57422339, compound

https://huagongshe.com/reaction/658617

Reaction equation

Participants

RoleNameHCIDCharge
ReactantPhenethylamineHCID 1001—
Reactant4-Methyloxybenzyl chlorideHCID 69993—
ReactantMethyl 4-(Chlorosulfonyl)benzoateHCID 4738388—
ProductHCID 57422339HCID 57422339—

Reaction Steps

Prepared as in example 5-10 from 2-phenylethanamine, methyl 4-(chlorosulfonyl)-benzoate (Example 5-10c) and 1-(chloromethyl)-4-methoxybenzene. MS (M−H, 424.1); 1H NMR (400 MHz, DMSO-d6): δ, ppm: 2.51 (m, 2H), 3.23 (m, 2H), 3.74 (s, 3H), 4.31 (s, 2H), 4.31 (s, 2H), 6.92 (m, 2H), 6.98 (m, 2H), 7.20-7.27 (m, 5H), 7.85 (m, 2H), 8.06 (m, 2H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08076491B2
Source datasetuspto-grants-2011_12
ORD IDord-44af309068144934a9b3e8246129be76
Source noteuspto-grants-2011_12