HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dibenzylamine → 4-(dibenzylsulfamoyl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dibenzylamine | HCID 7656 | — |
| Reactant | Methyl 4-(Chlorosulfonyl)benzoate | HCID 4738388 | — |
| Product | 4-(dibenzylsulfamoyl)benzoic acid | HCID 4552362 | — |
Reaction Steps
Prepared as in example 5-27 from dibenzylamine and methyl 4-(chlorosulfonyl)-benzoate (Example 5-10c). MS (M−H, 380.1); 1H NMR (400 MHz, DMSO-d6): δ, ppm: 4.52 (s, 4H), 7.10 (m, 4H), 7.25 (m, 6H), 8.00 (d, 2H, J=8.4 Hz), 8.15 (d, 2H J=8.4 Hz), 13.5 (s, broad, 1H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076491B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-244f8eed365a4fa4b805cff8dbc53a94 |
| Source note | uspto-grants-2011_12 |