HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 871814, compound → HCID 57944939, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 871814 | HCID 871814 | — |
| Reactant | Methyl 4-(Chlorosulfonyl)benzoate | HCID 4738388 | — |
| Product | HCID 57944939 | HCID 57944939 | — |
Reaction Steps
Prepared as in example 5-10 from N-(3,4-difluorobenzyl)(4-methoxyphenyl)-methanamine (example 5-36a) and methyl 4-(chlorosulfonyl)benzoate (example 5-10c). MS (M−H, 446); 1H NMR (400 MHz, DMSO-d6): δ ppm: 3.69 (s, 3H), 4.20 (s, 4H), 6.73 (d, J=8.8 Hz, 2H), 6.93 (m, 2H), 6.98 (d, J=8.8 Hz, 2H), 7.22 (m, 1H), 7.74 (d, J=8.4 Hz, 2H), 7.99 (d, J=8.4 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076491B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-93c2aa9a91934cdb8e0970ab0f6d15cc |
| Source note | uspto-grants-2011_12 |