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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 658635Generated: October 30, 2026

HCID 871814, compound → HCID 57944939, compound

https://huagongshe.com/reaction/658635

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 871814HCID 871814—
ReactantMethyl 4-(Chlorosulfonyl)benzoateHCID 4738388—
ProductHCID 57944939HCID 57944939—

Reaction Steps

Prepared as in example 5-10 from N-(3,4-difluorobenzyl)(4-methoxyphenyl)-methanamine (example 5-36a) and methyl 4-(chlorosulfonyl)benzoate (example 5-10c). MS (M−H, 446); 1H NMR (400 MHz, DMSO-d6): δ ppm: 3.69 (s, 3H), 4.20 (s, 4H), 6.73 (d, J=8.8 Hz, 2H), 6.93 (m, 2H), 6.98 (d, J=8.8 Hz, 2H), 7.22 (m, 1H), 7.74 (d, J=8.4 Hz, 2H), 7.99 (d, J=8.4 Hz, 2H).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08076491B2
Source datasetuspto-grants-2011_12
ORD IDord-93c2aa9a91934cdb8e0970ab0f6d15cc
Source noteuspto-grants-2011_12