HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzylamine → HCID 57944899, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzylamine | HCID 7504 | — |
| Reactant | 4-Methoxybenzaldehyde | HCID 31244 | — |
| Reactant | methyl 2-(4-(chlorosulfonyl)phenyl)acetate | HCID 23388822 | — |
| Product | HCID 57944899 | HCID 57944899 | — |
Reaction Steps
Prepared as in example 5-27 from Methyl 2-(4-(chlorosulfonyl)phenyl)acetate (example 5-47a), 4-methoxybenzaldehyde and benzylamine. MS (M−H, 424.10); 1H NMR (400 MHz, DMSO-d6): δ, ppm: 3.66 (s, 3H), 3.72 (s, 2H), 4.18 (s, 2H), 4.22 (s, 2H), 6.73 (d, J=8.4 Hz, 2H), 6.91 (d, J=8.4 Hz, 2H), 7.02 (m, 2H), 7.19 (m, 3H), 7.49 (d, J=8.4 Hz, 2H), 7.80 (d, J=8 Hz, 2H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076491B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-88a5e6c90266418787d3f60f7aef6193 |
| Source note | uspto-grants-2011_12 |