HuagongsheHuagongshe Chemistry Print Report · For research reference only
Isovanillin → 3-((tert-Butyldimethylsilyl)oxy)-4-methoxybenzaldehyde
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Isovanillin | HCID 12127 | — |
| Reactant | tert-Butyldimethylsilyl chloride | HCID 28928 | — |
| Product | 3-((tert-Butyldimethylsilyl)oxy)-4-methoxybenzaldehyde | HCID 359558 | 100% |
Reaction Steps
Prepared as in Example 12-1c from 3-hydroxy-4-methoxybenzaldehyde and tert-butylchlorodimethylsilane. Yield 100%, yellowish liquid. MS 267 (MH+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08076491B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-e48f70dc59ff4fdda07a021aee6fabac |
| Source note | uspto-grants-2011_12 |