Borane;tetrahydrofuran → HCID 57956759, compound

HRID 658887Notes

Reaction equation

HRID 658887 reaction equation
[OH:1][CH:2]([C:13]1[CH:18]=[CH:17][CH:16]=[C:15]([CH2:19][CH2:20][C:21]([OH:28])([CH2:25][CH2:26][CH3:27])[CH2:22][CH2:23][CH3:24])[CH:14]=1)[CH2:3][CH2:4][NH:5][C:6](=O)OC(C)(C)C.B.C1COCC1>>[OH:1][CH:2]([C:13]1[CH:14]=[C:15]([CH:16]=[CH:17][CH:18]=1)[CH2:19][CH2:20][C:21]([OH:28])([CH2:22][CH2:23][CH3:24])[CH2:25][CH2:26][CH3:27])[CH2:3][CH2:4][NH:5][CH3:6]

Participants

3

Reactant 2

HCID 2723981Borane;tetrahydrofuranHCID 57956786HCID 57956786, compound

Product 1

HCID 57956759HCID 57956759, compound

Procedure

Reduction of tert-butyl 3-hydroxy-3-(3-(3-hydroxy-3-propylhexyl)phenyl)propylcarbamate using BH3-THF gives Example 167.

Workup

  1. customgives Example 167

Sources & evidence

ORD record
ord-ecb99fb44fa84721a0e04f535f4060e0
Source dataset
uspto-grants-2011_12
Patent number
US08076516B2

Reaction notes

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