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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 659325Generated: October 31, 2026

Ethylamine → HCID 24852466, compound

https://huagongshe.com/reaction/659325

Reaction equation

Participants

RoleNameHCIDCharge
ReactantEthylamineHCID 6341—
ReactantHCID 24852685HCID 24852685—
ProductHCID 24852466HCID 248524663%

Reaction Steps

3-(1-Benzyl-2-oxo-1,2,3,4-tetrahydropyrido[2,3-b]pyrazin-7-yl)benzoic acid (35 mg) was coupled with ethylamine as in General Procedure 8 to give the title compound as a yellow solid (3% yield). LCMS: m/z=387.26 (M+H+), 1H-NMR (CDCl3, 400 MHz) δ 1.27 (3H, t, J=7.2 Hz), 3.47 (2H, quartet, J=7.2 Hz), 4.50 (2H, s), 5.28 (2H, s), 7.36 (8H, m), 7.48 (1H, t, J=7.6 Hz), 7.79 (2H, m), 7.84 (1H, s).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08080561B2
Source datasetuspto-grants-2011_12
ORD IDord-3b30abe493ad42f0a0c108e094789a7d
Source noteuspto-grants-2011_12