HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonia → 5-Chloro-2-methyl-6-sulfamoyl-1-indanone
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonia | HCID 222 | — |
| Reactant | 5-Chloro-6-chlorosulfonyl-2-methyl-1-indanone | HCID 22756381 | — |
| Product | 5-Chloro-2-methyl-6-sulfamoyl-1-indanone | HCID 22756406 | — |
Reaction Steps
According to Example 1 (d), the reaction of 5-chloro-6-chlorosulfonyl-2-methyl-1-indanone with liquid ammonia yields the raw product having a melting point of from 180° to 184° C. After recrystallization from ethanol, the compound melts at 190° to 192° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04129656 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-c9faffb31803428eb70b596ae6b5c989 |
| Source note | uspto-grants-1978_12 |