Sodium Cyanide → HCID 23683803, compound

HRID 65953Notes

Reaction equation

HRID 65953 reaction equation
[CH3:1][O:2][P:3]([N:7]([CH3:9])[CH3:8])([O:5]C)=[O:4].[C-]#N.[Na+:12]>CS(C)=O>[CH3:1][O:2][P:3]([N:7]([CH3:9])[CH3:8])([O-:5])=[O:4].[Na+:12]

Participants

4

Reactant 2

HCID 8929Sodium CyanideHCID 69003Dimethyl dimethylphosphoramidate

Product 1

HCID 23683803HCID 23683803, compound

Reagents, catalysts & solvents 1

HCID 679Dimethyl SulfoxideSolvent

Procedure

There is reacted with stirring for several hours at 60°-70° C. a mixture of 153 parts dimethyldimethylamidophosphate, 50 parts sodium cyanide and 400 parts dimethylsulphoxide (DMSO). The preparation is left overnight at ambient temperature, the product separated off by filtration, washed with DMSO and then with acetone and dried under vacuum. 140 parts of a white solid, readily soluble in water, are obtained.

Workup

  1. customThere is reacted
  2. customthe product separated off by filtration
  3. washwashed with DMSO
  4. dry with materialwith acetone and dried under vacuum
  5. custom140 parts of a white solid, readily soluble in water, are obtained

Sources & evidence

ORD record
ord-9fd2b65a771344edb613e1180d099c18
Source dataset
uspto-grants-1978_12
Patent number
US04129660

Reaction notes

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