反应详情

There is reacted with stirring for several hours at 60°-70° C. a mixture of 153 parts dimethyldimethylamidophosphate, 50 parts sodium cyanide and 400 parts dimethylsulphoxide (DMSO). The preparation is left overnight at ambient temperature, the product separated off by filtration, washed with DMSO and then with acetone and dried under vacuum. 140 parts of a white solid, readily soluble in water, are obtained.

1. customThere is reacted
2. customthe product separated off by filtration
3. washwashed with DMSO
4. dry with materialwith acetone and dried under vacuum
5. custom140 parts of a white solid, readily soluble in water, are obtained