HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → Prop-2-enenitrile--ethenylbenzene (1/1)
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | Styrene | HCID 7501 | — |
| Reactant | Acrylonitrile | HCID 7855 | — |
| Reactant | Tricalcium Phosphate | HCID 24456 | — |
| Solvent | Water | HCID 962 | — |
| Product | Prop-2-enenitrile--ethenylbenzene (1/1) | HCID 62696 | — |
Reaction Steps
A styrene-acrylonitrile copolymer resin (SAN) is synthesized by mixing 75 parts by weight styrene, 25 parts by weight acrylonitrile and 120 parts by weight deionized water; adding 0.2 parts by weight azo-bis-isobutyronitrile, 0.4 parts by weight tricalcium phosphate and 0.2 parts by weight mercaptan-based chain transfer agent to the above mixture; raising the temperature from room temperature to 80° C. for 90 minutes; and maintaining at this temperature for 180 minutes. The product is washed, dehydrated and dried to form a powder of the styrene-acrylonitrile copolymer resin (SAN).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08080619B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-1975b0950d324753ab8186cbd110ae31 |
| Source note | uspto-grants-2011_12 |