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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 659657Generated: October 30, 2026

Azobisisobutyronitrile → Prop-2-enenitrile--ethenylbenzene (1/1)

https://huagongshe.com/reaction/659657

Reaction equation

Participants

RoleNameHCIDCharge
ReactantAzobisisobutyronitrileHCID 6547—
ReactantStyreneHCID 7501—
ReactantAcrylonitrileHCID 7855—
ReactantTricalcium PhosphateHCID 24456—
SolventWaterHCID 962—
ProductProp-2-enenitrile--ethenylbenzene (1/1)HCID 62696—

Reaction Steps

A styrene-acrylonitrile copolymer resin (SAN) is synthesized by mixing 75 parts by weight styrene, 25 parts by weight acrylonitrile and 120 parts by weight deionized water; adding 0.2 parts by weight azo-bis-isobutyronitrile, 0.4 parts by weight tricalcium phosphate and 0.2 parts by weight mercaptan-based chain transfer agent to the above mixture; raising the temperature from room temperature to 80° C. for 90 minutes; and maintaining at this temperature for 180 minutes. The product is washed, dehydrated and dried to form a powder of the styrene-acrylonitrile copolymer resin (SAN).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08080619B2
Source datasetuspto-grants-2011_12
ORD IDord-1975b0950d324753ab8186cbd110ae31
Source noteuspto-grants-2011_12