HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86631538, compound → HCID 86631540, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86631538 | HCID 86631538 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86631540 | HCID 86631540 | 95% |
Reaction Steps
A stirred solution (0.2 M) of the product from example 1 step 1 in MeOH was added to 10% Pd on carbon (20% w/w) and the heterogeneous mixture was stirred under H2 (g) at RT overnight. Then, the reaction mixture was filtered through a pad of celite and washed with MeOH. Evaporation of the solvent yielded (95%) the title compound as a solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08080573B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-8021ecd14e0546cfa0bf5234e3a54bd7 |
| Source note | uspto-grants-2011_12 |