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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 659714Generated: October 30, 2026

HCID 86631538, compound → HCID 86631540, compound

https://huagongshe.com/reaction/659714

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 86631538HCID 86631538—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 86631540HCID 8663154095%

Reaction Steps

A stirred solution (0.2 M) of the product from example 1 step 1 in MeOH was added to 10% Pd on carbon (20% w/w) and the heterogeneous mixture was stirred under H2 (g) at RT overnight. Then, the reaction mixture was filtered through a pad of celite and washed with MeOH. Evaporation of the solvent yielded (95%) the title compound as a solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08080573B2
Source datasetuspto-grants-2011_12
ORD IDord-8021ecd14e0546cfa0bf5234e3a54bd7
Source noteuspto-grants-2011_12