HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 659811Generated: October 31, 2026
Dicyclopentadiene → 2-Propylbicyclo[2.2.1]hept-5-ene-2-carbaldehyde
https://huagongshe.com/reaction/659811
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Dicyclopentadiene | HCID 6492 | — |
| Reactant | 2-Methylenepentanal | HCID 70609 | — |
| Product | 2-Propylbicyclo[2.2.1]hept-5-ene-2-carbaldehyde | HCID 59559136 | 44.9% |
Reaction Steps
2-Methylene pentanal (302 g) and dicyclopentadiene (244 g) were loaded into a 2-L autoclave. The autoclave was sealed and heated to 170° C. The reaction was monitored by Gas Chromatography (“GC”) analysis, which showed the completion after 3 hours. The reaction was cooled to room temperature. The crude product was purified by distillation to yield 2-propylbicyclo[2.2.1]hept-5-ene-2-carbaldehyde (136 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US08080691B2 |
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| Source dataset | uspto-grants-2011_12 |
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| ORD ID | ord-7f73bcad4e404475af5ba45a780d13ae |
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| Source note | uspto-grants-2011_12 |
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