HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Dithionite → HCID 58150856, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Dithionite | HCID 24489 | — |
| Reactant | HCID 178428237 | HCID 178428237 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | Sodium Hydroxide | HCID 14798 | — |
| Product | HCID 58150856 | HCID 58150856 | — |
Reaction Steps
10 mg (0.04 mol) of 3-amino-2-chloro-4-[(4-hydroxyphenyl)imino]-6-methylcyclohexa-2,5-dien-1-one are added to a solution comprising 16 mg of sodium hydrosulphite in 500 μl of methanol and 5 μl of an aqueous sodium hydroxide solution. The reaction medium is stirred and then the solution is treated according to the usual procedure and characterized. 3-Amino-2-chloro-4-[(4-hydroxyphenyl)amino]-6-methylphenol (2a) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08083809B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-b81ee584f1824e92be6c82fa642a1d35 |
| Source note | uspto-grants-2011_12 |