Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Sodium Azide | HCID 33557 | — |
| Reactant | Azide | HCID 33558 | — |
| Reactant | HCID 86590825 | HCID 86590825 | — |
| Solvent | N,N-Dimethylformamide--water (1/1) | HCID 21962138 | — |
| Product | HCID 86590827 | HCID 86590827 | — |
Reaction Steps
Compound 87 (30 mg) was dissolved in DMF/water 1:1 (2 ml) and followed by sodium azide (26 mg, 10 equiv.). The reaction mixture stirred at 80° C. overnight. LCMS confirms conversion of starting material to product substituted with azide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08084458B2 |
|---|
| Source dataset | uspto-grants-2011_12 |
|---|
| ORD ID | ord-489d6bcf58b847b6888b5c430971c786 |
|---|
| Source note | uspto-grants-2011_12 |
|---|
