HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl 4-(4-nitrophenoxy)cyclohexanecarboxylate → HCID 178472464, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl 4-(4-nitrophenoxy)cyclohexanecarboxylate | HCID 57435335 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178472464 | HCID 178472464 | 100% |
Reaction Steps
Palladium (10 wt. %) on carbon (200 mg) was added in one portion to a solution of ethyl 4-(4-nitrophenoxy)cyclohexanecarboxylate (6.95 g, 23.7 mmol) in EtOH (200 mL) and the reaction mixture was stirred under a hydrogen atmosphere at ambient temperature for 16 h. The reaction mixture was filtered and concentrated in vacuo to leave the title compound as a yellow oil (6.24 g, 100%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08084478B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-7b20099fff9243b48475df16ec761391 |
| Source note | uspto-grants-2011_12 |