huagongshe.com
HRID660173

反应详情

EQUATION

反应方程式

HRID 660173 的结构方程式

REACTANTS

反应物

2
结构：CCS
HCID6343

Ethanethiol

C2H6S

结构：CCCCCSc1c[nH]nc1C1CN2CCC1CC2
HCID178447695

未命名化合物

PRODUCTS

生成物

1
结构：CCSc1c[nH]nc1C1CN2CCC1CC2
HCID178477307

未命名化合物

收率 30%

PROCEDURE

实验过程

Compound 49D was prepared following the procedure as described for the synthesis of compound 49B (see Scheme 10) using ethanethiol as reagent. Subsequent purification by flash chromatography (EtOH to EtOH/triethylamine 99/1) afforded compound 49D.

WORKUP

后处理

  1. customSubsequent purification by flash chromatography (EtOH to EtOH/triethylamine 99/1)