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HRID66032

反应详情

EQUATION

反应方程式

HRID 66032 的结构方程式

REACTANTS

反应物

3
结构：CCO
HCID702

Ethanol

C2H6O

结构：Nc1ccc(S(=O)(=O)O)c2cccc(S(=O)(=O)O)c12
HCID8336

1,5-Naphthalenedisulfonic acid, 4-amino-

C10H9NO6S2

结构：[Na+].[OH-]
HCID14798

Sodium Hydroxide

HNaO

PRODUCTS

生成物

1
结构：Nc1ccc(S(=O)(=O)[O-])c2cccc(S(=O)(=O)[O-])c12.[Na+].[Na+]
HCID44150211

Disodium 4-aminonaphthalene-1,5-disulfonate

C10H7NNa2O6S2

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

A 14.0 g amount of 4-amino-1,5-naphthalenedisulfonic acid is suspended in 100 ml of water and the solution is made basic with 5N sodium hydroxide. The solution is warmed and absolute ethyl alcohol is added until a solid is precipitated. The solid is collected by filtration and is washed with 85% aqueous ethyl alcohol, ethyl alcohol and ether, then dried in vacuo to yield 12.0 g of 4-amino-1,5-naphthalenedisulfonic acid disodium salt.

WORKUP

后处理

  1. temperatureThe solution is warmed
  2. customis precipitated
  3. filtrationThe solid is collected by filtration
  4. washis washed with 85% aqueous ethyl alcohol, ethyl alcohol and ether
  5. customdried in vacuo