Triethylamine → HCID 68920532, compound

Participants

Reaction Conditions

Reaction Steps

1-Phenylpropenone (58 mg, 0.44 mmol), 5-(2-benzyloxy-4-iodophenyl)-1,1-dioxo-2-(2-trimethylsilanylethyl)-1,2,5-thiadiazolidin-3-one (200 mg, 0.37 mmol), Pd(OAc)2 (4 mg), triethylamine (372 mg, 0.367 mmol), and acetonitrile (3 mL) are placed in a microwave vial and heated at 120° C. for 15 min. The mixture is filtered over Celite and washed with acetonitrile. The filtrate is evaporated to give the title compound which is used directly in the next step.

Provenance & Evidence