3-Butenylbenzene → HCID 24968959, compound

HRID 660515Notes

Reaction equation

HRID 660515 reaction equation
C([O:8][C:9]1[CH:14]=[C:13](I)[CH:12]=[CH:11][C:10]=1[N:16]1[S:20](=[O:22])(=[O:21])[N:19](CC[Si](C)(C)C)[C:18](=[O:29])[CH2:17]1)C1C=CC=CC=1.[CH2:30]([C:34]1[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=1)[CH2:31][CH:32]=[CH2:33]>>[OH:8][C:9]1[CH:14]=[C:13]([CH2:33][CH2:32][CH2:31][CH2:30][C:34]2[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=2)[CH:12]=[CH:11][C:10]=1[N:16]1[S:20](=[O:21])(=[O:22])[NH:19][C:18](=[O:29])[CH2:17]1

Participants

3

Reactant 2

HCID 130333-ButenylbenzeneHCID 667569375-(2-Benzyloxy-4-iodophenyl)-1,1-dioxo-2-(2-trimethylsilanylethyl)-1,2,5-thiadiazolidin-3-one

Product 1

HCID 24968959HCID 24968959, compound

Procedure

The title compound is prepared from 5-(2-benzyloxy-4-iodophenyl)-1,1-dioxo-2-(2-trimethylsilanylethyl)-1,2,5-thiadiazolidin-3-one and but-3-enyl-benzene analogous to Example 51: (M−1)−=359.

Sources & evidence

ORD record
ord-a5df9a984aba404da1ae16530e69d638
Source dataset
uspto-grants-2011_12
Patent number
US08084448B2

Reaction notes

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