HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 68837979, compound → HCID 68839644, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 68837979 | HCID 68837979 | — |
| Catalyst | Platinum | HCID 23939 | — |
| Product | HCID 68839644 | HCID 68839644 | — |
Reaction Steps
A mixture of (E)-3-{3-benzyloxy-4-[1,1,4-trioxo-5-(2-trimethylsilanylethyl)-1,2,5-thiadiazolidin-2-yl]-phenyl}-acrylic acid tert-butyl ester (485 mg, 0.89 mmol) and 5% platinum-on-carbon (50 mg) is stirred under an atmosphere of hydrogen for 5 h. The catalyst is filtered through Celite and solvent removed under reduced pressure to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08084448B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-71af0c13a56948ed870c0500f493e1e8 |
| Source note | uspto-grants-2011_12 |