Ethyl Acetate → HCID 68995192, compound

Participants

Reaction Conditions

Reaction Steps

To a solution of N-((1R*,2S*)-2-{3-Benzyloxy-4-[1,1,4-trioxo-5-(2-trimethylsilanylethyl)-1,2,5-thiadiazolidin-2-yl]-benzyl}-cyclohexyl)-methanesulfonamide (118 mg, 0.194 mmol) in DMF (3 mL) is added CsF (118 mg, 0.78 mmol) and the mixture is stirred at 90° C. for 1 h. Ethyl acetate is added and the mixture is washed with 1N HCl and brine. The organic phase is dried over magnesium sulfate and the solvent is removed under reduced pressure to give the title compound.

Provenance & Evidence