3-Buten-2-ol → HCID 57777287, compound

HRID 660715Notes

Reaction equation

HRID 660715 reaction equation
C([O:8][C:9]1[CH:14]=[C:13](I)[CH:12]=[CH:11][C:10]=1[N:16]1[S:20](=[O:22])(=[O:21])[NH:19][C:18](=[O:23])[CH2:17]1)C1C=CC=CC=1.[CH3:24][CH:25]([OH:28])[CH:26]=[CH2:27]>>[OH:8][C:9]1[CH:14]=[C:13]([CH2:27][CH2:26][CH:25]([OH:28])[CH3:24])[CH:12]=[CH:11][C:10]=1[N:16]1[S:20](=[O:21])(=[O:22])[NH:19][C:18](=[O:23])[CH2:17]1

Participants

3

Reactant 2

HCID 117163-Buten-2-olHCID 688386435-(2-Benzyloxy-4-iodophenyl)-1,1-dioxo-1,2,5-thiadiazolidin-3-one

Product 1

HCID 57777287HCID 57777287, compound

Procedure

The title compound is prepared from 5-(2-benzyloxy-4-iodophenyl)-1,1-dioxo-1,2,5-thiadiazolidin-3-one and but-3-en-2-ol analogous to Example 44: (M−1)−=299; HPLC retention time=1.16 min (method B)

Sources & evidence

ORD record
ord-244058c0682443fba1c742bc659d9bff
Source dataset
uspto-grants-2011_12
Patent number
US08084448B2

Reaction notes

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