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HRID660766

反应详情

EQUATION

反应方程式

HRID 660766 的结构方程式

REACTANTS

反应物

1
结构：COC(=O)CN(c1ccc(OCC(=O)OCC[Si](C)(C)C)cc1OCc1ccccc1)S(=O)(=O)NC(=O)OC(C)(C)C
HCID68997226

未命名化合物

PRODUCTS

生成物

1
结构：C[Si](C)(C)CCOC(=O)COc1ccc(N(CC(=O)O)S(N)(=O)=O)c(OCc2ccccc2)c1
HCID68842574

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：ClCCl.O=C(O)C(F)(F)F
溶剂HCID21863450

未命名化合物

PROCEDURE

实验过程

A solution of methyl N-(2-(benzyloxy)-4-{2-oxo-2-[2-(trimethylsilyl)ethoxy]ethoxy}phenyl)-N-{[(tert-butoxycarbonyl)amino]sulfonyl}glycinate (1.15 g, 1.84 mmol) in 20 mL of TFA/methylene chloride (1:1) is stirred at RT for 30 min. The solvent is removed under reduced pressure and the residue is dissolved in methylene chloride and the solvent evaporated (4×) to give the title compound.

WORKUP

后处理

  1. customThe solvent is removed under reduced pressure
  2. dissolutionthe residue is dissolved in methylene chloride
  3. customthe solvent evaporated (4×)