HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-(2-Benzyloxy-4-iodophenyl)-1,1-dioxo-2-(2-trimethylsilanylethyl)-1,2,5-thiadiazolidin-3-one → HCID 57777357, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-(2-Benzyloxy-4-iodophenyl)-1,1-dioxo-2-(2-trimethylsilanylethyl)-1,2,5-thiadiazolidin-3-one | HCID 66756937 | — |
| Reactant | HCID 86625049 | HCID 86625049 | — |
| Product | HCID 57777357 | HCID 57777357 | — |
Reaction Steps
The title compound is prepared from 5-(2-benzyloxy-4-iodophenyl)-1,1-dioxo-2-(2-trimethylsilanylethyl)-1,2,5-thiadiazolidin-3-one and methanesulfonic acid 2-iodomethylphenyl ester analogous to Example 306, steps C-F: (M−1)−=333. HPLC retention time=1.04 min (Method A).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08084448B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-db5e55c5017d4f76a1d5463b4414cbd5 |
| Source note | uspto-grants-2011_12 |