HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl formate → N-Formyl-p-(1-adamantyloxy)aniline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl formate | HCID 8025 | — |
| Reactant | 4-(1-Adamantyloxy)aniline | HCID 7289477 | — |
| Product | N-Formyl-p-(1-adamantyloxy)aniline | HCID 12510309 | — |
Reaction Steps
A suspension of 10.0 g. (0.041 mole) of p-(1-adamantyloxy)aniline in 60 ml. ethyl formate was stirred at reflux for 48 hours. The mixture was then taken to dryness and the residue recrystallized from Me2CO:cyclohexane. There was obtained 9.67 g. (87%) of the amide, N-formyl-p- (1-adamentyloxy)aniline m.p. 149°-150°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04130561 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-e9be8195b9ad443788f78dcb9649addf |
| Source note | uspto-grants-1978_12 |