HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 58116487, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 58116485 | HCID 58116485 | — |
| Product | HCID 58116487 | HCID 58116487 | 29.6% |
Reaction Steps
37.1 mg (0.123 mmol) of the compound from Example 51 were reacted according to General Method 2 with 38.3 mg (0.111 mmol) of meta-chloroperbenzoic acid. Enantiomer separation of 37.7 mg of the racemate according to Method 4D gave 16.1 mg of the title compound from Example 52 (enantiomer 1) and 16.5 mg of the title compound from Example 53 (enantiomer 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08084469B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-603ae2a41f204f43a59a388ca644f882 |
| Source note | uspto-grants-2011_12 |