HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 58116470, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 58116517 | HCID 58116517 | — |
| Product | HCID 58116470 | HCID 58116470 | 41.7% |
Reaction Steps
55.0 mg (0.128 mmol) of the compound from Example 55 were reacted according to General Method 2 with 39.7 mg (0.115 mmol) of meta-chloroperbenzoic acid. Enantiomer separation of 50.7 mg of the racemate according to Method 4D gave 22.1 mg of the title compound from Example 56 (enantiomer 1) and 21.4 mg of the title compound from Example 57 (enantiomer 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08084469B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-30810578765a42989be0e7de0daffc30 |
| Source note | uspto-grants-2011_12 |