HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 58116520, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | HCID 58116506 | HCID 58116506 | — |
| Product | HCID 58116520 | HCID 58116520 | 25.6% |
Reaction Steps
60.0 mg (0.122 mmol) of the compound from Example 59 were reacted according to General Method 2 with 38.0 mg (0.110 mmol) of meta-chloroperbenzoic acid. Enantiomer separation of 33.9 mg of the racemate according to Method 7D gave 15.6 mg of the title compound from Example 60 (enantiomer 1) and 13.4 mg of the title compound from Example 61 (enantiomer 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08084469B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-278c6a26a2184f7a9b4c674e26c06cc3 |
| Source note | uspto-grants-2011_12 |