HCID 67499044, compound → HCID 67499337, compound

HRID 661360Notes

Reaction equation

HRID 661360 reaction equation
[F:1][C:2]1([C:12]2[S:13][CH:14]=[CH:15][N:16]=2)[CH2:11][CH2:10][C:5]2(OCC[O:6]2)[CH2:4][CH2:3]1.ClC1C(C2(F)CCC3(OCCO3)CC2)=NC=CC=1>>[F:1][C:2]1([C:12]2[S:13][CH:14]=[CH:15][N:16]=2)[CH2:3][CH2:4][C:5](=[O:6])[CH2:10][CH2:11]1

Participants

3

Reactant 2

HCID 67499044HCID 67499044, compoundHCID 67499172HCID 67499172, compound

Product 1

HCID 67499337HCID 67499337, compound

Procedure

The title compound was prepared using the procedure as described in Example 1C, except for substituting the product of Example 20B for the product of Example 1B. 1H NMR (300 MHz, DMSO-d6) δ ppm 7.82-7.95 (m, 2 H), 2.61-2.72 (m, 6 H), 2.24-2.42 (m, 2 H). MS (DCI) m/e 200 (M+H)+.

Sources & evidence

ORD record
ord-04c3b1848ef0461499d53fb207c48ce5
Source dataset
uspto-grants-2011_12
Patent number
US08084616B2

Reaction notes

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