HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N-Dimethylethylenediamine → N-(2-(dimethylamino)ethyl)-2-methyl-7-oxo-4,5,6,7-tetrahydro-1H-indole-3-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N-Dimethylethylenediamine | HCID 66053 | — |
| Reactant | HCID 59376005 | HCID 59376005 | — |
| Product | N-(2-(dimethylamino)ethyl)-2-methyl-7-oxo-4,5,6,7-tetrahydro-1H-indole-3-carboxamide | HCID 66769068 | 80% |
Reaction Steps
Similar procedure as Example 2, 2-methyl-7-oxo-4,5,6,7-tetrahydro-1H-indole-3-carboxylic acid (S4) 0.2 g (1.0 mmol) and N1,N1-dimethylethane-1,2-diamine 0.19 g (2.1 mmol) was reacted to give 0.21 g (80%) of the titled compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08084621B2 |
| Source dataset | uspto-grants-2011_12 |
| ORD ID | ord-f2d51744eef747038ae4e467be01e547 |
| Source note | uspto-grants-2011_12 |