HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Oxobutanoic acid → 1-Piperidinium
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Oxobutanoic acid | HCID 1112 | — |
| Reactant | Piperidine | HCID 8082 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 1-Piperidinium | HCID 637969 | — |
| Product | 4-Oxobutanoate | HCID 9543238 | — |
Reaction Steps
100 Mg. of 4-(8-methoxy-6,11-dihydrodibenzo-[b.e.]-thiepin-11-one-3-yl)-4-oxobutyric acid in 10 ml. of benzene is treated with 60 mg. of piperidine. The solution obtained is allowed to stand for one hour and the crystalline material which forms is filtered, washed with ether and air dried to yield piperidinium 4-(8-methoxy-6,11-dihydrodibenzo-[b.e.]-thiepin-11-one-3-yl)-4-oxobutyrate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04130654 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-95cdf6991778486985518cab3455bb88 |
| Source note | uspto-grants-1978_12 |