HuagongsheHuagongshe Chemistry Print Report · For research reference only
P-Phenylenediamine → 1-Ethyl-3-methylpentyl-p-phenylenediamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | P-Phenylenediamine | HCID 7814 | — |
| Reactant | 5-Methyl-3-heptanone | HCID 7822 | — |
| Reactant | N,N'-bis(1-ethyl-3-methylpentyl)-p-phenylenediamine | HCID 94138 | — |
| Product | 1-Ethyl-3-methylpentyl-p-phenylenediamine | HCID 86736227 | — |
Reaction Steps
A mixture of 768 g. (6 moles) 5-methyl-3-heptanone and 108 g. (1 mole) p-phenylenediamine was reacted and worked up in the same manner as that of Example 1 to give 330 g. (99%) residue of crude N,N'-bis(1-ethyl-3-methylpentyl)-p-phenylenediamine product [IVa, R2 =C2H5, R3 =CH2CH(CH3)C2H5 ] containing some mono-Schiff's base III-c and some di-Schiff's base III-d.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04131622 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-e5b8fb6e2940468c85e1c9a250460137 |
| Source note | uspto-grants-1978_12 |