HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Chlorobutanoic acid → Tri-n-butyl(carboxypropyl)phosphonium Chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Chlorobutanoic acid | HCID 12300 | — |
| Reactant | Tributylphosphine | HCID 13831 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Tri-n-butyl(carboxypropyl)phosphonium Chloride | HCID 85918976 | — |
Reaction Steps
Tri-n-butyl phosphine (0.1 mole) and 4-chlorobutyric acid (0.1 mole) were refluxed in toluene for 4 hours. Evaporation of the solvent from the reaction mixture left a viscous liquid whose infrared spectrum and elemental analysis corresponded to a compound of the formula
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04131633 |
| Source dataset | uspto-grants-1978_12 |
| ORD ID | ord-c0497a2fdd6846519d384910679bcf61 |
| Source note | uspto-grants-1978_12 |