HRID66272

反应详情

EQUATION

反应方程式

HRID 66272 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

9,10-Dihydro-9,10-dimethylanthracene was prepared by hydrogenation of 9,10-dimethylanthracene with Girdler G-22 copper chromite catalyst in toluene at 120° C. and 1500 psi for 1 hour. The mixtures resulting from five such runs were combined and filtered, and the off-white solid product was isolated by evaporating the solvent. It was characterized by nmr spectroscopy.

WORKUP

后处理

  1. customThe mixtures resulting from five such runs
  2. filtrationfiltered
  3. customthe off-white solid product was isolated
  4. customby evaporating the solvent