HRID66370

反应详情

EQUATION

反应方程式

HRID 66370 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A mixture of 700 mg. of 2-(2-nitrophenyl)oxazolo[5,4-b]pyridine in 50 ml. of ethanol was hydrogenated over 150 mg. of 5% palladium on carbon catalyst. The catalyst was removed by filtration and the solvent was concentrated to dryness. The residue was recrystallized from chloroformpetroleum ether to give 2-(2-aminophenyl)oxazolo[5,4-b]pyridine, m.p. 142°-144° C.

WORKUP

后处理

  1. additionA mixture of 700 mg
  2. customThe catalyst was removed by filtration
  3. concentrationthe solvent was concentrated to dryness
  4. customThe residue was recrystallized from chloroformpetroleum ether