HRID66370
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A mixture of 700 mg. of 2-(2-nitrophenyl)oxazolo[5,4-b]pyridine in 50 ml. of ethanol was hydrogenated over 150 mg. of 5% palladium on carbon catalyst. The catalyst was removed by filtration and the solvent was concentrated to dryness. The residue was recrystallized from chloroformpetroleum ether to give 2-(2-aminophenyl)oxazolo[5,4-b]pyridine, m.p. 142°-144° C.
WORKUP
后处理
- additionA mixture of 700 mg
- customThe catalyst was removed by filtration
- concentrationthe solvent was concentrated to dryness
- customThe residue was recrystallized from chloroformpetroleum ether