HRID66428

反应详情

EQUATION

反应方程式

HRID 66428 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

To a reaction vessel fitted with an air-bleed tube, thermometer, stirrer, and condenser there are charged sulfopropionic anhydride (29.1 g.), 2-hydroxypropyl methacrylate (29.1 g.), the monomethyl ether of hydroquinone (0.1 g.) and toluene (60 g.). The mixture is stirred, sparged with dry air as in (1) above and heated. After 0.5 hour at 60° C. a solution containing 29% by weight of methacryloxyisopropyl sulfopropionate is obtained.

WORKUP

后处理

  1. customTo a reaction vessel fitted with an air-bleed tube
  2. customsparged
  3. dry with materialwith dry air as in (1) above
  4. temperatureheated
  5. additionAfter 0.5 hour at 60° C. a solution containing 29% by weight of methacryloxyisopropyl sulfopropionate
  6. customis obtained