HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 23700354, compound → 1-[3-Acetylthio-3-(5-chloro-2-thenoyl)-2-methylpropionyl]-L-proline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 23700354 | HCID 23700354 | — |
| Reactant | HCID 53880190 | HCID 53880190 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 1-[3-Acetylthio-3-(5-chloro-2-thenoyl)-2-methylpropionyl]-L-proline | HCID 54261225 | — |
Reaction Steps
Bromination of the [S]-1-[3-(5-chloro-2-thenoyl)-2-methylpropionyl]-L-proline and reaction of the brominated product with sodium thioacetate in acetonitrile gives a mixture of the [R-(R*,S*)] and [R-(R*,R*)] isomers of the product of the Example as a glass.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04342689 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-de4ce3fad7264a008d4de8ea7ef562bc |
| Source note | uspto-grants-1982_08 |