HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzenecarbothioic acid, sodium salt (1:1) → 1-[3-(Benzoylthio)-3-(5-chloro-2-thenoyl)propionyl]-L-proline
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzenecarbothioic acid, sodium salt (1:1) | HCID 23688990 | — |
| Reactant | 1-[3-bromo-3-(5-chloro-2-thenoyl)propionyl]-L-proline | HCID 54052188 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | 1-[3-(Benzoylthio)-3-(5-chloro-2-thenoyl)propionyl]-L-proline | HCID 53795252 | — |
Reaction Steps
As for Example 21, 0.01 mole of 1-[3-bromo-3-(5-chloro-2-thenoyl)propionyl]-L-proline is reacted with sodium thiobenzoate for 16 hours in acetonitrile to give the product of the Example as a glass.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04342690 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-bed49674223344e9a7fb86932611280b |
| Source note | uspto-grants-1982_08 |