HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → 3-Phenyl-3-(4-nitrophenyl)propenoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 3-(4-Nitrophenyl)-3-phenylprop-2-enoic acid | HCID 53427600 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 3-Phenyl-3-(4-nitrophenyl)propenoyl chloride | HCID 54529932 | — |
Reaction Steps
A mixture of 22 g. of 3-phenyl-3-(4-nitrophenyl)propenoic acid, 11.7 g. of thionyl chloride and 150 ml. of benzene was heated under reflux for 1 hour. The solvent was removed by evaporation in vacuo, and the residual solid was recrystallized from carbon tetrachloride. This afforded 20 g. of the title compound, m.p. 117°-120° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04342781 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-c9dc609ad93844f48364bf8bb6e0a502 |
| Source note | uspto-grants-1982_08 |