反应详情

In accordance with Reaction I of Example 1, 15.5 g. (0.1 mole) of 2-nitrothiophenol, 11.34 g. (0.12 mole) of 1-chloro-2-propanol, 4.0 g. (0.1 mole) of sodium hydroxide and 150 ml. of water were used for the reaction and an oily product was extracted with benzene after the reaction and benzene was distilled off after a dehydration to obtain 20.2 g. of blackish brawn liquid 2-(β-hydroxypropylthio)nitrobenzene (yield of 94.8%).

1. customIn accordance with Reaction I of Example 1, 15.5 g
2. extractionan oily product was extracted with benzene
3. customafter the reaction and benzene
4. distillationwas distilled off after a dehydration
5. customto obtain 20.2 g