HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
Dimethyl Sulfoxide → 4-Methylthio-m-tolyloxyacetonitrile
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | Dimethyl Sulfoxide | HCID 679 | — |
| Edukt | Chloroacetonitrile | HCID 7856 | — |
| Edukt | Potassium Carbonate | HCID 11430 | — |
| Edukt | 3,4-Xylenethiol | HCID 87799 | — |
| Produkt | 4-Methylthio-m-tolyloxyacetonitrile | HCID 70547184 | — |
Reaktionsschritte
The compound 4-methylthio-m-tolyloxyacetonitrile was prepared substantially as described in previous examples by heating a mixture of 55.0 g of 4-methylthio-m-cresol, 30 g of chloroacetonitrile, 70.7 g of anhydrous K2CO3 and 104 ml of DMSO, which gave 66.0 g of the compound as a reddish oil.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04343808 |
| Quelldatensatz | uspto-grants-1982_08 |
| ORD ID | ord-d13cad06f7ec4a42870381464c0daccd |
| Quellennotiz | uspto-grants-1982_08 |