huagongshe.com
HRID66811

反应详情

EQUATION

反应方程式

HRID 66811 的结构方程式

REACTANTS

反应物

3
结构：CCOC(=O)Cl
HCID10928

Ethyl chloroformate

C3H5ClO2

结构：CCCCCCCCCC(C)N
HCID114476

2-Undecanamine

C11H25N

结构：CC(=CC(=O)O)c1cccc([N+](=O)[O-])c1
HCID54402156

未命名化合物

PRODUCTS

生成物

1
结构：CCCCCCCCCC(C)NC(=O)C=C(C)c1cccc([N+](=O)[O-])c1
HCID53905448

未命名化合物

收率 72%

PROCEDURE

实验过程

The 3-(3-nitrophenyl)-2-butenoic acid from Preparation 12 having a melting point of 147°-149° C. was reacted with ethyl chloroformate, followed by 1-methyldecylamine, according to the procedure of Preparation 22. This afforded a 72% yield of the title product.

WORKUP

后处理

  1. customaccording to the procedure of Preparation 22