HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 20529127, compound → 2-Methyl-3-phenyl-1H-indole-4-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 20529127 | HCID 20529127 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 2-Methyl-3-phenyl-1H-indole-4-ol | HCID 20529161 | — |
Reaction Steps
An amount of 22.5 g (0.1 mole) of 4,5,6,7-tetrahydro-2-methyl-3-phenyl-1H-4indolone and 5 g of palladium on charcoal were heated for six hours to 200° C. After cooling, ether was added under stirring, and the mixture was filtered. The ether filtrate was evaporated, and the residue was chromatographed on silicagel (solvent: toluene).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04343811 |
| Source dataset | uspto-grants-1982_08 |
| ORD ID | ord-61be059a49c1429482ec4bc1c67b0b36 |
| Source note | uspto-grants-1982_08 |